In Situ TEM Solution
Triton AX
Heating & Cooling Liquid Electrochemical System for TEM
for TEM
Triton AX is the world's first system to enable simultaneous in situ electrochemical analysis at temperatures ranging from -50 °C to 300 °C. The temperature is completely user-definable to provide precise control over experimental conditions.
In Situ Liquid Cell: Triton
With complete solutions from sample preparation to reporting results, Triton AX brings a new level of operand conditions to TEM.
The first-of-its-kind machine vision software combined with the only thermoelectric liquid cooling system on the market enables a stable, precise, and quantitative temperature-controlled electrochemical solution.
This in situ solution can be used to enhance green energy research, and materials development and aid the analysis of dose-sensitive materials, for the study of batteries, corrosion and materials science, and more.
Perform temperature-dependent studies simultaneously with electrochemistry with Triton AX
Copper Dendrite Formation at 5 °C
STEM micrograph and cyclic voltammetry curve of Pt working electrode with copper plating layer at 5 °C. Dendrite morphology, kinetics, and current measurements differ significantly (smaller, slower, and lower, respectively) from those at higher temperatures (below). The inset shows the CV curve with a smaller Y-axis, demonstrating that even without visual changes, there is still a reaction occurring. The near-freezing temperature has slowed the reaction down significantly.
Copper sulfate electrolyte (50 mM) in sulfuric acid (0.1 M) flowing at 10 uL/hr.
Copper Dendrite Formation at 98 °C
STEM micrograph and cyclic voltammetry curve of Pt working electrode with copper plating layer at 98 °C. Dendrite morphology, kinetics, and current measurements differ significantly (larger, faster, and higher, respectively) from those at lower temperatures (above).
Copper sulfate electrolyte (50 mM) in sulfuric acid (0.1 M) flowing at 10 uL/hr.